Hach-lange ISENH318103 User Manual User Manual

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User Manual
DOC022.52
.80107
Ammonia Probe: Model ISENH318101 or ISENH318103
Safety information
Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the
instrument could occur if not observed. A symbol on the instrument is referenced in the
manual with a precautionary statement.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after
12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European
electrical equipment users must now return old or end-of-life equipment to the Producer for disposal at no charge to
the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return end-of-life
equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.
Specifications
Note: Specifications are subject to change without notice.
Specifications Details
Probe type Digital combination gas-sensing probe with a refillable outer body, double-
junction reference and a built-in temperature sensor
Range 0.01 mg/L (5x10
-7
M) to 14,000 mg/L (1 M) as NH
3
-N
Sample pH range > pH 11 per Ammonia ISA
Linear region 0.5 mg/L to 14,000 mg/L as NH
3
-N
Slope 57 mV/decade (90 to 110% in linear range at 25 °C (77 °F) per Nernstian
theoretical value)
Operating temperature range 5 to 50 °C (41 to 122 °F)
Storage temperature range 5 to 35 °C (41 to 95 °F)
Junction Double junction (annular)
Reference type Ag/AgCl
Fill solution 3 M KCl gel (non-refillable), 0.1 M NH
4
Cl (outer body, refillable)
Membrane Replaceable Hach ISENH3181 Ammonia membrane module
Response time in linear region < 60 seconds (application dependent)
Minimum sample volume 15 mL
Minimum immersion depth 25.4 mm (1 in.)
Dimensions Diameter: 12 mm (0.47 in.)
Length: 175 mm (6.89 in.)
Cable length: 1 or 3 m (3.28 or 9.84 ft)
Cable connection M12 digital output and connector compatible with HQd meters
Product overview
The ISENH318101 or ISENH318103 probe is a digital combination gas-sensing electrode
with a refillable outer body, double-junction reference and built-in temperature sensor
(Figure 1). The probe is available with a 1 or 3 m (3.28 or 9.84 ft) cable and is intended
for laboratory use. The probe measures ammonia concentration in water samples.
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Summary of Contents

Page 1 - User Manual

User ManualDOC022.52.80107Ammonia Probe: Model ISENH318101 or ISENH318103Safety informationPrecautionary labelsRead all labels and tags attached to th

Page 2 - Calibration

6. Select Acceptance Criteria and update the settings:Option DescriptionAcceptance Limits Sets the tolerance limits for check standard—1% to 20%.Cal E

Page 3

Note: After long-term storage, the ISENH3181 probe (with membrane module assembled)might need to be conditioned in Ammonia probe storage solution for

Page 4 - Measurement—direct method

Message or symptom Possible cause ActionDrifting/inaccurate readingsDirty sensing element Clean the probe (body, membrane module and glassbulb).Clogge

Page 5

Message or symptom Possible cause ActionTemperature out of rangeCalibration temperature value isoutside of rangeMake sure that the sample temperature

Page 6 - Run a check standard

• V1 = spike volume (mL)•V2 = spike volume (mL) + 25 mL sample volume• E = expected concentration of spike (mg/L)• R = percent recovery• A = actual re

Page 7 - Advanced operation

Figure 1 Probe overview1 Soaker bottle 5 1 or 3 m (3.28 or 9.84 ft) cable2 Membrane module protector cap (3x) 6 Fill solution bottle3 Membr

Page 8 - Change calibration options

Calibration notes:•Stir the standards and samples at a slow and steady rate to prevent the formation ofa vortex.• Additional standard sets along with

Page 9 - Change check standard options

6. Add a stir barand put the probein the firststandard solutionin the set. Do notput the probe onthe bottom orsides of thecontainer.7. Put the beake

Page 10 - Maintenance

• The integrated temperature sensor and HQd meter software do not compensate fordifferences in temperature between calibration standards and samples.

Page 11 - Troubleshooting

InterferencesThe sensing element responds to ammonia as well as other ions. Typically, proberesponse to another ion increases the potential, and cause

Page 12

Advanced operationParameter-specific settings can be changed through the Full Access Options menu.Details about menu navigation, available options and

Page 13

Option DescriptionAuto Stabilization Sets auto stabilization—on (default) or off.The default stability drift rate is 1.0 mV/min.Stability Criteria Whe

Page 14 - 05/2013, Edition 5

Option DescriptionMinimum CalPointsSets the minimum number of calibration points necessary before acalibration can be completed—2 or 3.Slope Limit Set

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